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1, 1′ -Thiocarbonyldiimidazole; CAS6160-65-2

Colour
Yellow
Samples
Available
Purity
99%
Certificates
ISO9001/SGS
Package
1kg/5kg/10kg/25kg
Stocks
in Stock
Lead Time
5-7 Working Days
Shelf Life
2-3 Years
Site Audit
Available
Transport
Air/Express/Sea
MOQ
10g
Transport Package
Drum/Bottle/Bags
Trademark
Yunbang
Origin
China
Reference Price
Please contact us for quote
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Product Description

1,1'-Thiocarbonyldiimidazole;CAS  6160-65-2
 
1, 1′ -Thiocarbonyldiimidazole; CAS6160-65-2
 
1,1'-Thiocarbonyldiimidazole Chemical Properties
Melting point  98-102 °C(lit.)
Boiling point  342°C (rough estimate)
density  1.3046 (rough estimate)
refractive index  1.5500 (estimate)
storage temp.  2-8°C
solubility  Soluble in terahydrofuran, tolu ene and dichloro meth ane.
pka 1.96±0.10(Predicted)
form  Powder
color  Bright yellow
Water Solubility  decomposes
Sensitive  Moisture Sensitive
BRN  609349
Stability: Stable, but air and moisture sensitive. Incompatible with strong oxidizing agents, strong acids.
InChIKey RAFNCPHFRHZCPS-UHFFFAOYSA-N
CAS DataBase Reference 6160-65-2(CAS DataBase Reference)
 
Safety Information
Hazard Codes  Xi
Risk Statements  22-34
Safety Statements  22-24/25-45-36/37/39-26
WGK Germany  3
F  9-21
Hazard Note  Irritant/Keep Cold/Moisture Sensitive
HS Code  29332900
 
1,1'-Thiocarbonyldiimidazole Usage And Synthesis
Chemical Properties yellow powder
Uses 1,1'Thiocarbonyldiimidazole can be used to deoxygenate carboxylic monosaccharide analogues.
Uses 1,1'-Thiocarbonyldiimidazole is used as a reagent for the deoxygenation of alcohols with tributyltin hydride and diols with lithium aluminum hydride. It is also used to deoxygenate carboxylic monosaccharide analogues. Further, it is a useful reagent involved in biochemical synthesis. In addition to this, it is used to prepare 1-[bis-(4-methoxy-phenyl)-methyl]-1H-imidazole by reacting with 4,4'-dimethoxy-benzhydrol.
Synthesis Reference(s) The Journal of Organic Chemistry, 43, p. 337, 1978  DOI:   10.1021/jo00396a035
Purification Methods It forms yellow crystals on recrystallisation from tetrahydro fur an or by sublimation at 10-3torr (bath temperature 70-80o). It is hydrolysed by H2O and should be stored dry. [Staab & Walther Justus Liebigs Ann Chem 657 98 1962; Pullukat et al. Tetrahedron Lett 1953 1967, Hanessian et al. Can J Chem 65 1859 1987, Rajanbabu et al. J Am Chem Soc 111 1759 1989.] Thiochrome {2,7-dimethyl-5H -thiachromine-8-ethanol; 3,8-dimethyl-2-hydroxyethyl-5H -
 
1, 1′ -Thiocarbonyldiimidazole; CAS6160-65-2
 
1, 1′ -Thiocarbonyldiimidazole; CAS6160-65-2 1, 1′ -Thiocarbonyldiimidazole; CAS6160-65-2 1, 1′ -Thiocarbonyldiimidazole; CAS6160-65-2
Company Informations:

Hunan Yunbang Pharmaceutical Co., Ltd. ( Yunbangpharm) located in Changsha High-tech Industrial Park, Hunan. It is a high-tech enterprise specializing in the research and development, production and sales of Pharmaceutical raw materials, Pharmaceutical intermediates(API) and Fine chemicals. Based in China, Yunbangpharm has been providing suitable solutions for many domestic,foreign pharmaceutical companies and traders. Excellent quality, good reputation and authentic price have won the praise of the majority of customers.
The company adheres to the corporate tenet of "We do not produce medicines, but help pharmaceutical companies make good medicines".

We can provide customers with customized processing, research and development services;
We can develop high-end Pharmaceutical and chemical products with high technical difficulties,high barriers and unique production processes;
We can provide 100 grams Grade, kilograms, and hundred kilograms of raw material pharmaceutical intermediates and other products.
We can perform -100°C to 300°C reaction.

R&D strength is the company's core competitiveness.Yunbangpharm has maintains a good cooperation relationship with many Universities and Research institutes locally, which can quickly transform R&D results into industrial production.

Our goal : To achieve the integrated upgrade of P harmaceutical intermediates, raw materials and high-end chemical products, adhere to "serving pharmaceutical companies, creating our brands" to provide customers with high-quality and low-cost pharmaceutical and chemical products, realizing Win-win cooperation and common development.

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